A Modified-One Pot Synthesis of Diaminoglyoxime
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Abstract:
The one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. By increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).
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a modified-one pot synthesis of diaminoglyoxime
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Journal title
volume 23 issue 1
pages 117- 118
publication date 2004-04-01
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